About Dma storage modulus rises at high temperature
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6 FAQs about [Dma storage modulus rises at high temperature]
What is tensile storage modulus (DMA)?
(a) Tensile storage modulus (b) loss factor (tan δ) versus temperature and (c) Tg versus reciprocal Mn of the polyimides. DMA is an effective and sensitive method to determine Tg of polyimide and the DSC curve is shown in the supplementary information (Figure S2).
How can DMA detect a viscoelastic variable?
DMA can detect and analyze viscoelastic variables like storage modulus, loss modulus, and loss tangent, as well as their dependence on temperature and frequency. The Tg and the temperature dependency of the modulus can both be studied via temperature dispersion measurements.
What does heat set temperature look like in a DMA?
Depending on its strength, the heat set temperature can also be seen in the DMA. While it is normally seen in either a TMA or a Constant Gauge Length (CGL) experiment, it will sometimes appear as either a sharp drop in storage modulus (E ′) or an abrupt change in probe position.
What is the effect of DMA on a dynamic cooling segment?
Fig. 7. DMA results for the dynamic cooling segment (180 °C to 25 °C) following the experiment in Fig. 3 (after 20 min at 180 °C). The distinct increase in the storage modulus, accompanied by a decrease in the loss modulus at cooling, is a consequence of a partially seen rubber-glass transition.
How does modulus affect a polymer chain entanglement?
modulus (Ge) is correlated with the polymer chain entanglement.If the polymer is partially crosslinked, then i s molten state will not be observed in a temperature ramp test. After Tg, the rubbery plateau area will extend p to higher temperatures until the polymer starts to decompose. Figure 3 shows an example temperat
How does DMA temperature affect crosslinking?
ferent amounts of crosslinking using a DMA in the tension mode. As can be seen from the graph, the measured rubbery plate u modulus increased with increasing the degree of crosslinking. In the meantime, the gl observed o shift to higher temperatures.2Temperature T (oC)Figure 4. DMA temperature ramp te
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